GSO OIML R113:2008
OIML R 113:1994
Gulf Standard
Current Edition
·
Approved on
20 February 2008
Portable gas chromatographs for field measurements of hazardous chemical pollutants
GSO OIML R113:2008 Files
English
28 Pages
Current Edition
Reference Language
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GSO OIML R113:2008 Scope
1.1 This International Recommendation provides procedures for testing and verifying
the performance of a portable gas chromatograph (GC) for use in measuring potentially
hazardous chemical pollutants associated with hazardous waste sites as mandated
by national laws and regulations. This Recommendation does not intend to exclude
any other equivalent means of measurement or analysis of such pollutants. A portable
instrument is self-contained, or an integrated compact assembly that is capable of carrying
out a complete analysis on site and operates on battery power; however, it may
have the option of operating on alternating current (AC) power. Several types of portable
gas chromatographs that employ a range of techniques for introducing samples
and for detecting individual compounds of interest are available. The major components
specified in this Recommendation reflect examples of current technology and are
not intended to exclude new developments. Laboratory based GCs are covered in the
OIML International Recommendation R 82 Gas chromatographs for measuring pollution
from pesticides and other toxic substances.
1.2 Sample components of interest for detection by a portable GC are components that
can pass through its column in detectable amounts without undergoing significant
irreversible adsorption or decomposition and which can be detected. Examples of general
compound types of hazardous chemical pollutants that may be detected by a portable
GC are listed in Annex A.
l.3 Sampling plans, sample preparation, and measurement methods are beyond the
scope of this Recommendation.
1.4 Instruments that meet the requirements of this Recommendation have flexibility in
some major components depending on their specific application. The following such
components are covered:
• direct air sampling devices and syringe injection devices for either gaseous or liquid
samples;
• packed and capillary columns operating under fixed or adjustable temperature control;
• packed and capillary columns operating at ambient temperature and under certain
other environmental conditions;
• photoionization detectors (PID), flame ionization detectors (FID), argon ionization
detectors (AID), and electron capture detectors (ECD).
Note: The detectors mentioned above have the broadest applicability and therefore
those most commonly used in field applications. Other detectors may be appropriate
and may also meet the requirements of this Recommendation for specific
applications.
1.5 Instrument performance better than the criteria prescribed for these applications
may be achieved by optimizing the performance of each major component of the
measuring system. In such cases, success depends on the knowledge, skill, and experience
of the operator.
1.6 This Recommendation does not address requirements and tests for instruments
which may be necessary for personal safety. Therefore, users should determine
whether the instruments meet the safety and labeling requirements specified in national
regulations
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